Determination of valproic acid and 3-heptanone in plasma using air-assisted liquid-liquid microextraction with the assistance of vortex: Application in the real samples

Behruz Feriduni ¹, Mohammad Barzegar ², Shahram Sadeghvand ³, Shadi Shiva ⁴, Maryam Khoubnasabjafari ⁵ , Abolghasem Jouyban ^1,6 *

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2- Pourshamsi T, Amri F, Abniki M. A comprehensive review on application of the syringe in liquid- and solid-phase microextraction methods. J IRAN CHEM SOC. 2021;18(2):245 [Crossref]

3- Fang Z, Zhang H, Guo J, Guo J. Overview of therapeutic drug monitoring and clinical practice. Talanta. 2024;266:124996 [Crossref]

4- Mohammadi P, Masrournia M, Es'haghi Z, Pordel M. Determination of four antiepileptic drugs with solvent assisted dispersive solid phase microextraction – Gas chromatography–mass spectrometry in human urine samples. Microchemical Journal. 2020;159:105542 [Crossref]

5- Azooz E, Al-Wani H, Gburi M, Al-Muhanna E. Recent modified air-assisted liquid–liquid microextraction applications for medicines and organic compounds in various samples: A review. 2022;20(1):525 [Crossref]

6- Naseri N, Kharrazi S, Abdi K, Alizadeh R. Fabrication of an SPME fiber based on ZnO@GA nanorods coated onto fused silica as a highly efficient absorbent for the analysis of cancer VOCs in water and urine. Analytica Chimica Acta. 2021;1183:338983 [Crossref]

7- Farajzadeh M, Mohebbi A, Pazhohan A, Nemati M, Afshar Mogaddam M. Air–assisted liquid–liquid microextraction; principles and applications with analytical instruments. TrAC Trends in Analytical Chemistry. 2020;122:115734 [Crossref]

8- Lipska K, Gumieniczek A, Pietraś R, Filip A. HPLC-UV and GC-MS Methods for Determination of Chlorambucil and Valproic Acid in Plasma for Further Exploring a New Combined Therapy of Chronic Lymphocytic Leukemia. Molecules. 2021;26(10):2903 [Crossref]

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